HRID2273652
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
This compound was prepared, starting from compound 76 (0.15 g, 0.30 mmol), according to the procedure developed for compound 11. Reaction time at room temperature: 12 h to give compound 77 (157 mg, 0.28 mmol) as a very hygroscopic beige solid. Yield 91%; mp 143-145° C.; IR (KBr) ν 1291, 1456, 1559, 1675, 2500-3600 cm−1; ESI-MS m/z 497.9 [M+H]+.
WORKUP
后处理
- customThis compound was prepared
- customReaction time at room temperature