Hydrogen Sulfide → HCID 57879252, compound

HRID 2273825Notes

Reaction equation

HRID 2273825 reaction equation
[C:1]([O:12][CH3:13])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10].[SH2:14]>CCCCC>[SH:14][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][C:1]([O:12][CH3:13])=[O:11]

Participants

4

Reactant 2

HCID 402Hydrogen SulfideHCID 1778877Methyl 9-decenoate

Product 1

HCID 57879252HCID 57879252, compound

Reagents, catalysts & solvents 1

HCID 8003PentaneSolvent

Procedure

The resulting methyl 9-decenoate (156 g) is placed in a photochemical reactor comprising a reaction loop, with 100 g of pentane and 60 molar equivalents of liquefied hydrogen sulfide (1806 g condensed at 20° C. under a pressure of 17.5 bar).

Sources & evidence

ORD record
ord-af8bc7c210e84f398d80a5edea731b8f
Source dataset
uspto-grants-2015_09
Patent number
US09126919B2

Reaction notes

Loading…