Chlorosuccinimide → HCID 68357732, compound

HRID 2274009Notes

Reaction equation

HRID 2274009 reaction equation
[Cl:1][C:2]1[C:3]([C:13]2(Cl)[CH2:15][CH2:14]2)=[N:4][N:5]([CH3:12])[C:6]=1[C:7]([O:9][CH2:10][CH3:11])=[O:8].[F:17]C1(C2C=C(C(OCC)=O)N(C)N=2)CC1.ClN1C(=O)CCC1=O>>[Cl:1][C:2]1[C:3]([C:13]2([F:17])[CH2:15][CH2:14]2)=[N:4][N:5]([CH3:12])[C:6]=1[C:7]([O:9][CH2:10][CH3:11])=[O:8]

Participants

4

Reactant 3

HCID 31398ChlorosuccinimideHCID 68326381HCID 68326381, compoundHCID 68326403HCID 68326403, compound

Product 1

HCID 68357732HCID 68357732, compound

Procedure

The preparation was carried out analogously to the preparation of ethyl 4-chloro-3-(1-chlorocyclopropyl)-1-methyl-1H-pyrazole-5-carboxylate using ethyl 3-(1-fluorocyclopropyl)-1-methyl-1H-pyrazole-5-carboxylate and 3 eq of N-chlorosuccinimide

Sources & evidence

ORD record
ord-c0d7a5b4fc2a439e8177390389b5ba52
Source dataset
uspto-grants-2015_09
Patent number
US09126945B2

Reaction notes

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