HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 86666943, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | 4'',5''-DICHLORO-2''-HYDROXYACETOPHENONE | HCID 13850167 | — |
| Product | HCID 86666943 | HCID 86666943 | 71% |
Reaction Steps
The desired compound was prepared according to the procedure of Example 6, Step 2, using 1-(4,5-dichloro-2-hydroxyphenyl)ethanone and N-iodosuccinimide (instead of N-bromosuccinimide) as the starting materials in 71% yield. LCMS for C8H6Cl2IO2 (M+H)+: m/z=330.9, 332.9. Found: 330.8, 332.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126948B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-d55cd3a16d5e435bbc71460c8a9c92da |
| Source note | uspto-grants-2015_09 |