HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Diethoxyethylamine → HCID 178467947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Reactant | HCID 71001839 | HCID 71001839 | — |
| Catalyst | Cuprous chloride | HCID 62652 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 178467947 | HCID 178467947 | — |
Reaction Steps
0.38 g (2.86 mmol) of aminoacetaldehyde diethylacetal and 0.155 g (1.57 mmol) of CuCl were added to 0.48 .g (1.43 mmol) of 2-amino-1-ethyl-7-iodo-4-oxo-1,4-dihydro-quinoline-3-carbonitrile dissolved in 20 ml of DME. The solution was stirred and irradiated with microwaves for 0.5 hour at 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126972B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-f8e96bfddc3d4002819b45695c2008d0 |
| Source note | uspto-grants-2015_09 |