HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Diethoxyethylamine → HCID 67304207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Reactant | 4-Quinolinecarboxaldehyde | HCID 78072 | — |
| Product | HCID 67304207 | HCID 67304207 | 109.3% |
Reaction Steps
According to the procedure described in the synthesis method of Compound IX-2 with the modification that the reaction was carried out overnight, 2,2-diethoxyethanamine (3.64 ml, 25 mmol) was reacted with 4-quinolinecarboxaldehyde (3.14 g, 20 mmol) to obtain the title compound (6.0 g, 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126981B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-9fea1c88afea4c89af188799718df710 |
| Source note | uspto-grants-2015_09 |