HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 178419954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 1-(Bromomethyl)naphthalene | HCID 137844 | — |
| Reactant | HCID 178527937 | HCID 178527937 | — |
| Product | HCID 178419954 | HCID 178419954 | — |
Reaction Steps
1 (0.33 g, 1.5 mmol), TEA (0.209 mL, 1.5 mmol) and naphtylmethylbromide (0.332 g, 1.5 mmol) were dissolved in 10 mL of EtOH and kept under reflux overnight. The solvent was removed and the remaining oil was purified by flash-chromatography on silica gel, applying a CHCl3/MeOH gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126987B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-6777432e34b040faa3a0989362d225c4 |
| Source note | uspto-grants-2015_09 |