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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2274723Generated: October 31, 2026

Allyl bromide → HCID 178460816, compound

https://huagongshe.com/reaction/2274723

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAllyl bromideHCID 7841—
ReactantHCID 178527937HCID 178527937—
SolventEthanolHCID 702—
ProductHCID 178460816HCID 178460816—

Reaction Steps

1 (0.33 g, 1.5 mmol), TEA (0.209 mL, 1.5 mmol) and allylbromide (0.093 mL, 1.5 mmol) were dissolved in 10 mL of EtOH and kept under reflux overnight. The solvent was removed and the remaining oil was purified by flash-chromatography on silica gel, applying a CHCl3/MeOH gradient.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09126987B2
Source datasetuspto-grants-2015_09
ORD IDord-5db6ee4eb82f43789011c42c87141df0
Source noteuspto-grants-2015_09