HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 178460816, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | HCID 178527937 | HCID 178527937 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178460816 | HCID 178460816 | — |
Reaction Steps
1 (0.33 g, 1.5 mmol), TEA (0.209 mL, 1.5 mmol) and allylbromide (0.093 mL, 1.5 mmol) were dissolved in 10 mL of EtOH and kept under reflux overnight. The solvent was removed and the remaining oil was purified by flash-chromatography on silica gel, applying a CHCl3/MeOH gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126987B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-5db6ee4eb82f43789011c42c87141df0 |
| Source note | uspto-grants-2015_09 |