HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentafluorobenzyl bromide → HCID 178505969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentafluorobenzyl bromide | HCID 74484 | — |
| Reactant | HCID 178527937 | HCID 178527937 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178505969 | HCID 178505969 | — |
Reaction Steps
1 (0.33 g, 1.5 mmol), TEA (0.209 mL, 1.5 mmol) and pentafluorobenzylbromide (0.204 mL, 1.5 mmol) were dissolved in 10 mL of EtOH and kept under reflux overnight. The solvent was removed and the remaining oil was purified by flash-chromatography on silica gel, applying a CHCl3/MeOH gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09126987B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b7eb2551479d4f00aeff6a0ac217c30a |
| Source note | uspto-grants-2015_09 |