HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2275419Generated: October 30, 2026
Methanol → Methyl 2-fluoro-3-iodo-4-methylbenzoate
https://huagongshe.com/reaction/2275419
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Fluoro-3-iodo-4-methylbenzoic acid | HCID 59383900 | — |
| Product | Methyl 2-fluoro-3-iodo-4-methylbenzoate | HCID 67211177 | — |
Reaction Steps
In a 500 ml one-neck flask equipped with a magnetic stir-bar and condenser was added 2-fluoro-3-Iodo-4-methyl-benzoic acid (31.5 g, 112.5 mmol), 250 ml of methanol and 10 ml of sulfuric acid. The reaction was heated at 90° C. overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09127024B2 |
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| Source dataset | uspto-grants-2015_09 |
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| ORD ID | ord-f2ac138954ce499280eedf966c53f0fa |
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| Source note | uspto-grants-2015_09 |
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