HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57437974, compound → Ethyl 4-amino-5-methylpyridine-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57437974 | HCID 57437974 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 4-amino-5-methylpyridine-3-carboxylate | HCID 46735270 | 98.4% |
Reaction Steps
0.50 g of material prepared in Step A was dissolved in 15 mL of ethanol. 0.15 g of 10% palladium on carbon was added. The reaction mixture was placed under one atmosphere of hydrogen for 2 hours. The catalyst was removed by filtration. The solvent was removed with a rotary evaporator to afford 0.43 g of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560564B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-476daa395cd641c88469a6ece3beb246 |
| Source note | uspto-grants-2009_07 |