HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 67181984, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 5-amino-6-methylpyrimidine-4-carboxylate | HCID 45082623 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67181984 | HCID 67181984 | — |
Reaction Steps
2.0 g (12 mmol) of the material from Step E was dissolved in 24 mL of methanol. 12 mL of 1N solution of sodium hydroxide was added. After 1 hour the solvent was removed with a rotary evaporator. The residue was dried in a vacuum oven overnight to afford 2.39 g of the title compound as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560564B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-a18f5eba47124dc4a61e54ba6defff76 |
| Source note | uspto-grants-2009_07 |