HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 49852656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 49852657 | HCID 49852657 | — |
| Product | HCID 49852656 | HCID 49852656 | — |
Reaction Steps
TLC(CH2Cl2:MeOH, 92:8 v/v): Rf=0.55; UV/vis λmax 262 nm, 432 nm; HRMS (m/z): [M]+ calculated for C16H12O3S, 285.0585. found 285.0578. See Table 2 for NMR data. Roseobacticide B. TLC(CH2Cl2:MeOH, 92:8 v/v): Rf=0.58; UV/vis λmax 262 nm, 316 nm, 430 nm; HRMS (m/z): [M]+calculated for C16H12O2S, 269.0637. found 269.0635. See Table 3 for NMR data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09131687B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-2d0648749ab64e85b1257753d797e1b7 |
| Source note | uspto-grants-2015_09 |