HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → N-{[3-(Trifluoromethyl)phenyl]methylidene}hydroxylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-(Trifluoromethyl)benzaldehyde | HCID 67990 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Product | N-{[3-(Trifluoromethyl)phenyl]methylidene}hydroxylamine | HCID 2777383 | 93.5% |
Reaction Steps
In a similar manner as described in Preparation Example 1, by using 3-(trifluoromethyl)benzaldehyde (34.82 g, 200.0 mmol), sodium hydroxide (12.00 g, 300.0 mmol) and hydrochloric acid hydroxylamine (16.68 g, 240 mmol), a white solid required compound (35.33 g, 187 mmol, 93%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132126B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-49dfc682bb7a436ca053255ec074e786 |
| Source note | uspto-grants-2015_09 |