HRID2276395

反应详情

EQUATION

反应方程式

HRID 2276395 反应方程式

PROCEDURE

实验过程

In a similar manner as described in Preparation Example 1, by using 3-(trifluoromethyl)benzaldehyde (34.82 g, 200.0 mmol), sodium hydroxide (12.00 g, 300.0 mmol) and hydrochloric acid hydroxylamine (16.68 g, 240 mmol), a white solid required compound (35.33 g, 187 mmol, 93%) was obtained.

WORKUP

后处理

  1. customIn a similar manner as described in Preparation Example 1