HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 86210273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | p-Trifluoromethoxybenzaldehyde oxime | HCID 2777199 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86210273 | HCID 86210273 | 90.3% |
Reaction Steps
In a similar manner as described in Preparation Example 9, by using dimethylformamide (240 mL), 4-(trifluoromethoxy)benzaldehydeoxime (20.0 g, 97.51 mmol) and N-chlorosuccinimide (14.31 g, 107.26 mmol), a pale yellow solid required compound (21.10 g, 88.04 mmol, 90%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132126B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b2301dcff302406cbc7db282e258aaae |
| Source note | uspto-grants-2015_09 |