HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 85444714, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | N-{[3-(Trifluoromethyl)phenyl]methylidene}hydroxylamine | HCID 2777383 | — |
| Product | HCID 85444714 | HCID 85444714 | 95.3% |
Reaction Steps
In a similar manner as described in Preparation Example 9, by using 3-(trifluoromethyl)benzaldehydeoxime (30.0 g, 158.60 mmol), dimethylformimide (300 mL) and N-chlorosuccinimide (23.31 g, 174.46 mmol), a pale yellow solid required compound (33.81 g, 151.22 mmol, 95%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132126B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-effc0f617b554d6eb8c35d8b4945467d |
| Source note | uspto-grants-2015_09 |