Methyl cyanoacetate → HCID 70980612, compound

Participants

Reaction Steps

In a similar manner as described in Preparation Example 17, by using methanol (160 mL), N-hydroxy-3-(trifluoromethyl)benzimidoylchloride (8.00 g, 33.39 mmol), methylcyanoacetate (4.14 g, 41.74 mmol) and sodium methoxide (3.61 g, 66.78 mmol), a white solid required compound (7.46 g, 26.06 mmol, 78%) was obtained.

Provenance & Evidence