HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 70980423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86709607 | HCID 86709607 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70980423 | HCID 70980423 | 71.2% |
Reaction Steps
In a similar manner as described in Preparation Example 25, by using methanol (60 mL), 5-amino-3-(2-(trifluoromethyl)phenyl)isoxazol-4-carboxylate (6.0 g, 20.96 mmol) and 3% sodium hydroxide aqueous solution (60 mL), a white solid required compound (4.06 g, 14.92 mmol, 71%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132126B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-42e1eb8975754849854421222566b292 |
| Source note | uspto-grants-2015_09 |