HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 70980823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 70981025 | HCID 70981025 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70980823 | HCID 70980823 | 76% |
Reaction Steps
In a similar manner as described in Preparation Example 25, by using methanol (60 mL), methyl-5-amino-3-(4-(trifluoromethoxy)phenyl)isoxazol-4-carboxylate (6.0 g, 19.85 mmol) and 3% sodium hydroxide aqueous solution (60 mL), a white solid required compound (4.32 g, 15.02 mmol, 76%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132126B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-460a87952bc741e4a45e2598aa2be29e |
| Source note | uspto-grants-2015_09 |