HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 70982325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 70981114 | HCID 70981114 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70982325 | HCID 70982325 | 73% |
Reaction Steps
In a similar manner as described in Preparation Example 25, by using methanol (60 mL), methyl 5-amino-3-(3-(trifluoromethoxy)phenyl)isoxazol-4-carboxylate (6.0 g, 19.85 mmol) and 3% sodium hydroxide aqueous solution (60 mL), a white solid required compound (4.16 g, 14.43 mmol, 73%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09132126B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-95e95bc10b914c1da6a35c62dadc53fa |
| Source note | uspto-grants-2015_09 |