HuagongsheHuagongshe Chemistry Print Report · For research reference only
[3-Chloro-5-(trifluoromethyl)-2-pyridinyl][(diphenylmethylene)amino]acetonitrile → Amino[3-chloro-5-(trifluoromethyl)-2-pyridinyl]acetonitrile hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [3-Chloro-5-(trifluoromethyl)-2-pyridinyl][(diphenylmethylene)amino]acetonitrile | HCID 22988174 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Amino[3-chloro-5-(trifluoromethyl)-2-pyridinyl]acetonitrile hydrochloride | HCID 23078241 | — |
Reaction Steps
15.0 g of [3-chloro-5-(trifluoromethyl)-2-pyridinyl][(diphenylmethylene)amino]acetonitrile (0.037 mol) are stirred at room temperature for 3 h in a mixture of dichloromethane (15 mL) and hydrochloric acid 10% (15 mL). Phases are separated and the organic phase is washed with 15 mL of hydrochloric acid 10%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560567B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-1ec84a41e86c408e96c02642d9290f8c |
| Source note | uspto-grants-2009_07 |