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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2276621Generated: October 25, 2026

Bromobenzene → 1-Pentadecyl-3-phenoxybenzene

https://huagongshe.com/reaction/2276621

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBromobenzeneHCID 7961—
ReactantDimethylacetamideHCID 31374—
ReactantHydrogenated cardanolHCID 68146—
ReactantPotassiumHCID 5462222—
SolventWaterHCID 962—
Product1-Pentadecyl-3-phenoxybenzeneHCID 17747909—

Reaction Conditions

Temperature150 °C

Reaction Steps

Into the round bottom flask containing potassium salt of 3-pentadecyl phenol is added bromobenzene followed by Cu powder and in a solvent, DMAc (dimethyl acetamide). The reaction mixture is heated at 150° C. for 6 h. After completion of the reaction, the obtained dark colored reaction mixture is poured into water and the Cu salts are removed by filtration. The filtrate is extracted in a solvent, washed with water and dried, purified to obtain arylated product, 1-pentadecyl-3-phenoxybenzene.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09133089B2
Source datasetuspto-grants-2015_09
ORD IDord-098d7520d0d44e888b6a85333b30fb9f
Source noteuspto-grants-2015_09