HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2276621Generated: October 25, 2026
Bromobenzene → 1-Pentadecyl-3-phenoxybenzene
https://huagongshe.com/reaction/2276621
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Bromobenzene | HCID 7961 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Reactant | Hydrogenated cardanol | HCID 68146 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-Pentadecyl-3-phenoxybenzene | HCID 17747909 | — |
Reaction Steps
Into the round bottom flask containing potassium salt of 3-pentadecyl phenol is added bromobenzene followed by Cu powder and in a solvent, DMAc (dimethyl acetamide). The reaction mixture is heated at 150° C. for 6 h. After completion of the reaction, the obtained dark colored reaction mixture is poured into water and the Cu salts are removed by filtration. The filtrate is extracted in a solvent, washed with water and dried, purified to obtain arylated product, 1-pentadecyl-3-phenoxybenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09133089B2 |
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| Source dataset | uspto-grants-2015_09 |
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| ORD ID | ord-098d7520d0d44e888b6a85333b30fb9f |
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| Source note | uspto-grants-2015_09 |
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