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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2276622Generated: October 26, 2026

Dimethyl Sulfoxide → Anisole, m-pentadecyl-

https://huagongshe.com/reaction/2276622

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyl SulfoxideHCID 679—
ReactantMethyl iodideHCID 6328—
ReactantSodium HydroxideHCID 14798—
ReactantHydrogenated cardanolHCID 68146—
SolventWaterHCID 962—
ProductAnisole, m-pentadecyl-HCID 578947—

Reaction Steps

To a two necked round bottomed flask with a reflux condenser is added 3-pentadecyl phenol, DMSO, sodium hydroxide followed by dropwise addition of alkylating agent such as methyl iodide with constant stirring at room temperature. The stirring is continued for about 6-8 hrs. The reaction mixture is then poured into deionized water and the organic matter is extracted in diethyl ether, separated the organic layer, washed with water and dried, purified to obtain 3-pentadecyl anisole.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09133089B2
Source datasetuspto-grants-2015_09
ORD IDord-0cadd41262b44dd289521f0f2f868abf
Source noteuspto-grants-2015_09