HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → Anisole, m-pentadecyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Hydrogenated cardanol | HCID 68146 | — |
| Solvent | Water | HCID 962 | — |
| Product | Anisole, m-pentadecyl- | HCID 578947 | — |
Reaction Steps
To a two necked round bottomed flask with a reflux condenser is added 3-pentadecyl phenol, DMSO, sodium hydroxide followed by dropwise addition of alkylating agent such as methyl iodide with constant stirring at room temperature. The stirring is continued for about 6-8 hrs. The reaction mixture is then poured into deionized water and the organic matter is extracted in diethyl ether, separated the organic layer, washed with water and dried, purified to obtain 3-pentadecyl anisole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133089B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-0cadd41262b44dd289521f0f2f868abf |
| Source note | uspto-grants-2015_09 |