2-Amino-3-Hydroxypyridine → HCID 22486224, compound

HRID 227665Notes

Reaction equation

[C:1]([CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])#[N:2].N[C:22]1[C:27]([OH:28])=[CH:26][CH:25]=[CH:24][N:23]=1>>[O:28]1[C:27]2[C:22](=[N:23][CH:24]=[CH:25][CH:26]=2)[N:2]=[C:1]1[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

Reactant 2

HCID 281142-Amino-3-Hydroxypyridine

HCID 98566Nonadecanonitrile

Product 1

HCID 22486224HCID 22486224, compoundYield 30%

Procedure

This material was prepared in 30% yield from 1-cyanooctadecane (Mangold, H. K., et al., (1976) Chem. Phys. Lipids 17, 176-181) and 2-amino-3-hydroxypyridine using Method C3: mp 84-85° C.

Sources & evidence

ORD record: ord-07afa1d2bc074a1aafdce988781493cc
Source dataset: uspto-grants-2009_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07560570B2

Reaction notes

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