HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2276709Generated: October 30, 2026
4-Bromobenzoic acid → 4-Bromobenzoyl chloride
https://huagongshe.com/reaction/2276709
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Bromobenzoic acid | HCID 11464 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 4-Bromobenzoyl chloride | HCID 68515 | 97.3% |
Reaction Steps
A mixture of 4-bromobenzoic acid (8 g, 39.8 mmoL) in SOCl2 (80 mL) was stirred at 80° C. for 4 hours and then concentrated under reduce pressure. The resulting white solid was used directly for next step without further purification (8.5 g, yield 97.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09133105B2 |
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| Source dataset | uspto-grants-2015_09 |
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| ORD ID | ord-271086b9d52f4ec0bd8ff95c961c0878 |
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| Source note | uspto-grants-2015_09 |
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