HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67296040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67296116 | HCID 67296116 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67296040 | HCID 67296040 | 70% |
Reaction Steps
A 1,4-dioxane solution of 4N hydrochloric acid (5 mL) was added to N-[(1R)-1-(4-fluoronaphthalen-1-yl)ethyl]-2-methylpropane-2-sulfinamide (527 mg, 2.2 mmol), and the mixture was stirred for 30 minutes at room temperature. The precipitate generated was filtered, washed with ether, and was then dried under reduced pressure to give the title compound (358 mg, 70%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133140B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-ae31bc4e1971455daac926d556d75a8e |
| Source note | uspto-grants-2015_09 |