HuagongsheHuagongshe Chemistry Print Report · For research reference only
(R)-tert-butyl 3-hydroxy-3-(3-hydroxyphenyl)propylcarbamate → HCID 90405419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (R)-tert-butyl 3-hydroxy-3-(3-hydroxyphenyl)propylcarbamate | HCID 90405310 | — |
| Reactant | HCID 90405497 | HCID 90405497 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 90405419 | HCID 90405419 | — |
Reaction Steps
Condensation between ethyl 3-(thiophen-2-ylmethoxy)benzoate and acetonitrile following the method used in the preparation of phenol (Intermediate I) gave after flash column chromatography 3-oxo-3-(3-(thiophen-2-ylmethoxy)phenyl)propanenitrile as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133154B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-d1be2a4367ea4d1b9b9083a525eb1d8c |
| Source note | uspto-grants-2015_09 |