HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57755841, compound → HCID 57755851, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57755841 | HCID 57755841 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57755851 | HCID 57755851 | — |
Reaction Steps
To a solution of (3-Fluoro-phenyl)-(5-nitro-1H-indazol-3-yl)-amine (0.36 g, 1.3 mmol) in methanol (10 ml) was added 10% Pd/C (72 mg). The mixture was allowed to stir at room temperature under H2 atmosphere. After TLC showed the starting material to be consumed, the reaction was passed through a plug of celite. The filtrate was concentrated to give the title compound as an off-white solid. MS (ESI) m/z=243 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560467B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-7076824491ec4c438911c90e1744d6ca |
| Source note | uspto-grants-2009_07 |