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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 227728Generated: October 30, 2026

HCID 57755841, compound → HCID 57755851, compound

https://huagongshe.com/reaction/227728

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57755841HCID 57755841—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 57755851HCID 57755851—

Reaction Steps

To a solution of (3-Fluoro-phenyl)-(5-nitro-1H-indazol-3-yl)-amine (0.36 g, 1.3 mmol) in methanol (10 ml) was added 10% Pd/C (72 mg). The mixture was allowed to stir at room temperature under H2 atmosphere. After TLC showed the starting material to be consumed, the reaction was passed through a plug of celite. The filtrate was concentrated to give the title compound as an off-white solid. MS (ESI) m/z=243 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07560467B2
Source datasetuspto-grants-2009_07
ORD IDord-7076824491ec4c438911c90e1744d6ca
Source noteuspto-grants-2009_07