Hydrochloric Acid → HCID 86731412, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of tert-butyl (2-(benzyloxy)-5-(methoxymethoxy)pyridin-4-yl)carbamate (11.0 g) in THF (10 mL) and 6 M hydrochloric acid (30 mL) was stirred at 60° C. for 8 hr. The reaction mixture was cooled to 0° C., and the precipitate was collected by filtration, and washed with hexane. The obtained solid was dried under reduced pressure to give the title compound (5.87 g).

Provenance & Evidence