HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 57755825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | PyBroP | HCID 2733179 | — |
| Reactant | 6-Methyl-2-oxo-4-[4-(trifluoromethyl)phenyl]-1,2,3,4-tetrahydropyrimidine-5-carboxylic acid | HCID 53482105 | — |
| Reactant | HCID 69067693 | HCID 69067693 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57755825 | HCID 57755825 | — |
Reaction Steps
The titled compound was prepared following the procedure of Example 175 using 6-Methyl-2-oxo-4-(4-trifluoromethyl-phenyl)-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid, N3-(3,5-difluoro-phenyl)-1H-indazole-3,5-diamine, PyBroP and diisopropylethylamine in methylene chloride. MS (ESI) m/z=543 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560467B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-ca989b87fa7942c1b3ce86c2e8db93d2 |
| Source note | uspto-grants-2009_07 |