huagongshe.com
HRID2277472

反应详情

EQUATION

反应方程式

HRID 2277472 的结构方程式

REACTANTS

反应物

2
结构：N#Cc1ccnc(Cl)c1
HCID568638

2-Chloro-4-cyanopyridine

C6H3ClN2

结构：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1cn(C(c2ccccc2)(c2ccccc2)c2ccccc2)cn1
HCID11828117

4-(Tributylstannyl)-1-tritylimidazole

C34H44N2Sn

PRODUCTS

生成物

1
结构：N#Cc1ccnc(-c2cn(C(c3ccccc3)(c3ccccc3)c3ccccc3)cn2)c1
HCID90407660

未命名化合物

收率 77%

PROCEDURE

实验过程

The title compound was prepared in 77% yield from 2-chloro-4-pyridinenitrile and 4-(tributylstannyl)-1-tritylimidazole according to the procedure for Example 1, part A. 1H NMR (400 MHz, DMSO-d6): δ 7.17 (5H, m), 7.40-7.47 (10H, m), 7.49 (1H, d, J=1.2 Hz), 7.62 (1H, d, J=1.3 Hz), 7.65 (1H, dd, J=1.5 Hz and 5.0 Hz), 8.13 (1H, s), 8.67 (1H, d, 5.0 Hz).