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HRID2277484

反应详情

EQUATION

反应方程式

HRID 2277484 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1ccnc(Cl)c1
HCID2736842

Methyl 2-chloroisonicotinate

C7H6ClNO2

结构：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1cn(C(c2ccccc2)(c2ccccc2)c2ccccc2)cn1
HCID11828117

4-(Tributylstannyl)-1-tritylimidazole

C34H44N2Sn

PRODUCTS

生成物

1
结构：COC(=O)c1ccnc(-c2cn(C(c3ccccc3)(c3ccccc3)c3ccccc3)cn2)c1
HCID90407274

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from methyl 2-chloropyridine-4-carboxylate and 4-(tributylstannyl)-1-tritylimidazole according to the procedure for Example 1. 1H NMR (400 MHz, DMSO-d6): δ 3.92 (3H, s), 7.16 (5H, m), 7.38-7.46 (11H, m), 7.60 (1H, d, J=1.3 Hz), 7.64 (1H, dd, J=1.6 Hz and 5.0 Hz), 8.32 (1H, s), 8.64 (1H, d, 5.0 Hz).