Bis(2-chloroethyl) ether → HCID 90407394, compound

HRID 2277489Notes

Reaction equation

HRID 2277489 reaction equation
[NH:1]1[CH:5]=[C:4]([C:6]2[CH:11]=[C:10]([C:12]#[N:13])[CH:9]=[CH:8][N:7]=2)[N:3]=[CH:2]1.[Cl:14][CH2:15][CH2:16][O:17][CH2:18][CH2:19]Cl>>[Cl:14][CH2:15][CH2:16][O:17][CH2:18][CH2:19][N:1]1[CH:5]=[C:4]([C:6]2[CH:11]=[C:10]([C:12]#[N:13])[CH:9]=[CH:8][N:7]=2)[N:3]=[CH:2]1

Participants

3

Reactant 2

HCID 8115Bis(2-chloroethyl) etherHCID 178510201HCID 178510201, compound

Product 1

HCID 90407394HCID 90407394, compound

Procedure

The title compound was prepared from 2-(1H-imidazol-4-yl)pyridine-4-carbonitrile and bis(2-chloroethyl)ether according to the procedure for the preparation of Example 43, part A. [M+H] Calc'd for C13H13ClN4O, 278. Found, 277, 279.

Sources & evidence

ORD record
ord-d31f93e4c3d8483c9600e4c47e0d9436
Source dataset
uspto-grants-2015_09
Patent number
US09133166B2

Reaction notes

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