HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Butanesultam → HCID 86679166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Butanesultam | HCID 303508 | — |
| Reactant | 3-Bromo-5-(chloromethyl)pyridine | HCID 11701259 | — |
| Product | HCID 86679166 | HCID 86679166 | — |
Reaction Steps
In analogy to the procedure described for the preparation of intermediates B-1 [B], [1,2]thiazinane 1,1-dioxide has been coupled to 3-bromo-5-chloromethyl-pyridine (intermediate B-1 [A]) to yield the title compound as off-white solid. MS: 305.1, 307.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133158B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b34e1340c2ab42e8af5b385e118a96c2 |
| Source note | uspto-grants-2015_09 |