HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 89677025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 3-Chloro-2-fluorobenzaldehyde | HCID 736335 | — |
| Product | HCID 89677025 | HCID 89677025 | — |
Reaction Steps
The title compound was synthesized from 3-chloro-2-fluorobenzaldehyde and pyrrolidine as described in Example 67, Step 1 (800 mg, 30%). 1H NMR 300 MHz (CDCl3) δ 10.36 (s, 1H), 7.71-7.73 (m, 1H), 7.59-7.61 (m, 1H), 7.18-7.26 (m, 1H), 3.33-3.42 (m, 4H), 2.01-2.10 (m, 4H). LCMS (ESI, m/z): 210 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133148B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-bad290b96ebf42cabc90acfd00607935 |
| Source note | uspto-grants-2015_09 |