Hydrochloric Acid → HCID 89525783, compound

Participants

Reaction Conditions

Reaction Steps

N-[1-(4-bromothiophen-2-yl)-2-{[tert-butyl(dimethyl)silyl]oxy}ethyl]-2-methylpropane-2-sulfinamide (660 mg, 1.5 mmol) was dissolved in MeOH (15 mL) and the solution was cooled to 0° C., after which HCl (1.87 mL of a 4M solution in dioxane, 7.49 mmol) was added and the mixture was stirred for 120 minutes. The solvents were removed by coevaporation with toluene.

Provenance & Evidence