HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 131733469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | N,N-dimethylformamide N,N-dimethylacetamide | HCID 22628260 | — |
| Reactant | HCID 89739001 | HCID 89739001 | — |
| Product | HCID 131733469 | HCID 131733469 | — |
Reaction Steps
The product of Step 2 (13 g, 53 mmol) and pyrrolidine (2.3 mL) in DMF/DMA (150 ml) were heated at reflux overnight. The mixture was cooled and then concentrated to give the crude title compound, which was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133180B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-2db6cc5975e64e0c8c6765a7e888c0d6 |
| Source note | uspto-grants-2015_09 |