Dimethylformamide dimethyl acetal → HCID 67513546, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 1-(2-methyl-3-furanyl)-2-(2-methyl-4-pyridinyl)ethanone (0.430 g, 2.000 mmol) in N,N-dimethylformamide dimethyl acetal (0.266 ml, 2 mmol) was heated at 100° C. for 2 hours. The mixture was cooled to room temperature and the solvent was evaporated to give the title compound (540 mg) which was used crude in the next step. LC/MS [M+H]+=271.

Provenance & Evidence