HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 58449398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 58449365 | HCID 58449365 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58449398 | HCID 58449398 | — |
Reaction Steps
A round bottom flask was charged with methyl 3-(5-methylpyridin-2-yl)-5-(3-oxomorpholino)benzoate (50 mg, 0.15 mmol), methanol (1.2 mL) and lithium hydroxide (11 mg, 0.46 mmol) and the reaction mixture was stirred at room temperature for 1 h. The reaction mixture was acidified to pH=5 and concentrated under reduced pressure to get the title compound-LiCI mixture as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133122B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-21141de6d3f1442b89a2ad517e57d420 |
| Source note | uspto-grants-2015_09 |