Lithium Hydroxide → HCID 58449374, compound

Participants

Reaction Conditions

Reaction Steps

A round bottom flask was charged with methyl 3-bromo-5-(5-methylpyridin-2-yl)benzoate (300 mg, 0.98 mmol), tetrahydrofuran (15 mL) and lithium hydroxide (70 mg, 2.94 mmol). The reaction mixture was stirred at 50° C. overnight, and then filtered through sodium sulfate. The filtrate was concentrated under reduced pressure to afford the product as a white solid.

Provenance & Evidence