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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2278880Generated: November 1, 2026

HCID 46912313, compound → HCID 46912316, compound

https://huagongshe.com/reaction/2278880

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 46912313HCID 46912313—
CatalystManganese dioxideHCID 14801—
SolventDichloromethaneHCID 6344—
ProductHCID 46912316HCID 4691231640%

Reaction Steps

MnO2 (439 mg, 5.04 mmol) was added to a solution of 1-(6-amino-9-methyl-8-[1,2,3]triazol-2-yl-9H-purin-2-yl)butan-1-ol (51 mg, 0.2 mmol) in DCM (4 ml) at RT. The resulting heterogeneous solution was stirred overnight. After filtration over a celite pad, the solvent was removed under reduced pressure to afford the desired product as a white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09133197B2
Source datasetuspto-grants-2015_09
ORD IDord-58e9b14bd777454bb02dc512d26441ff
Source noteuspto-grants-2015_09