HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → HCID 90426063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 2-Chloroethyl isocyanate | HCID 16035 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 90426063 | HCID 90426063 | 100% |
Reaction Steps
A solution of methoxyethylamine (0.40 mL, 4.60 mmol) in THF (15 mL) was treated with 2-chloroethylisocyanate (0.35 mL, 4.10 mmol), stirred at RT for 3 h and concentrated to dryness to afford 1-(2-chloroethyl)-3-(2-methoxyethyl)urea (100% yield assumed) as a white solid. MS (ESI) m/z: 181.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133183B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-1a78d46a840746a48e97daebbdf163df |
| Source note | uspto-grants-2015_09 |