Hydrochloric Acid → HCID 178501523, compound

Participants

Reaction Steps

78 mg of {4-[6-(4-Methoxymethoxy-phenyl)-3-methyl-1-(tetrahydro-pyran-2-yl)-1H-pyrazolo[3,4-b]pyridin-4-ylmethyl]-2,2,5,5-tetramethyl-piperazin-1-yl}-acetic acid methyl ester were reacted with hydrochloric acid (4M in dioxane) and the volatiles were removed after 5 h. After purification by preparative HPLC 14 mg (21%) of the title compound were obtained.

Provenance & Evidence