HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68294268, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68294558 | HCID 68294558 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68294268 | HCID 68294268 | — |
Reaction Steps
A solution of 128 (400 mg, 1.30 mmol) and 4 N HCl in dioxane (4 mL) was stirred for 1 h. The reaction was concentrated to afford crude 2-(isopropylamino)-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidin-5-ol hydrochloride (130) which was used without additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133187B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-f011169cea54430f81947d3631002776 |
| Source note | uspto-grants-2015_09 |