Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thioacetamide | HCID 2723949 | — |
| Reactant | 2-Cyanopyrimidine | HCID 2757979 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | Pyrimidine-2-carbothioamide | HCID 23273397 | — |
Reaction Steps
A mixture of 2-cyanopyrimidine (15 g) and thioacetamide (20 g) in 100 mL of 10% concentrated HCl in Miff is heated with stirring at 90° C. for three hours and cooled. The solid is collected by filtration, washed with water and dried to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09133204B2 |
|---|
| Source dataset | uspto-grants-2015_09 |
|---|
| ORD ID | ord-ce581895d9db4aed93601a301b61095a |
|---|
| Source note | uspto-grants-2015_09 |
|---|
