HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23139185, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1793069-27-8 | HCID 88975469 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 23139185 | HCID 23139185 | 98% |
Reaction Steps
To a solution of tert-butyl 2-(4-formylpyrazol-1-yl)acetate (0.67 g, 3.19 mmol) in dioxane (10 mL) was added a 4N solution of HCl in dioxane (10 mL) and the mixture was stirred at room temperature for three days. The solvent was removed by evaporation under reduced pressure to afford the title compound (0.41 g, 98%) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09133185B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-10429221aa0a4db19a04a6f84c8f3332 |
| Source note | uspto-grants-2015_09 |