HRID2279936

反应详情

EQUATION

反应方程式

HRID 2279936 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of (R)—(R)-quinuclidin-3-yl2-((tert-butoxycarbonyl)amino)-2-phenylacetate I-46 (0.608 g, 1.687 mmol) in anhydrous dioxane (6 mL) was added with 2M HCl in ether (5.2 mL, 10.4 mmol). The reaction mixture was stirred at room temperature for 20 h. The solvent was removed in vacuo to afford the title compound as a white solid (0.564 g, quantitative yield).

WORKUP

后处理

  1. customThe solvent was removed in vacuo