HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 178488695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 3-(3-Fluoro-4-methoxyphenyl)-3-oxopropanenitrile | HCID 24726813 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178488695 | HCID 178488695 | — |
Reaction Steps
3-(3-Fluoro-4-methoxyphenyl)-3-oxopropanenitrile (2.13 g, 11 mmol) and hydrazine (0.38 mL, 12.13 mmol) were combined in absolute ethanol and the reaction mixture was heated to reflux overnight. Then, the solvent and excess hydrazine were evaporated to provide the title compound in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139532B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-c71eed9bdec84c09b2f888bcfd93972a |
| Source note | uspto-grants-2015_09 |