HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2281080Generated: November 4, 2026
Dimethylformamide dimethyl acetal → HCID 75201679, compound
https://huagongshe.com/reaction/2281080
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | HCID 56973649 | HCID 56973649 | — |
| Product | HCID 75201679 | HCID 75201679 | — |
Reaction Steps
A mixture of 17.0 g (79.1 mmol) 2-amino-4-bromo-6-fluoro-benzonitrile and 140 ml of N,N-dimethylformamide dimethyl acetal is heated to 120° C. for 2 h. After cooling RT the solvent is evaporated and the residual taken up in diethyl ether, filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09139577B2 |
|---|
| Source dataset | uspto-grants-2015_09 |
|---|
| ORD ID | ord-20915ce2c7c34cc79ed323c87645e781 |
|---|
| Source note | uspto-grants-2015_09 |
|---|
